Circular No. 30/2010/TT-BYT the national technical regulation for fluid milk products đã được thay thế bởi Circular 03/2017/TT-BYT QCVN 5-1:2017/BYT National technical regulation for fluid milk product và được áp dụng kể từ ngày 01/03/2018.
Nội dung toàn văn Circular No. 30/2010/TT-BYT the national technical regulation for fluid milk products
MINISTRY OF HEALTH | SOCIALIST REPUBLIC OF VIETNAM |
No. 30/2010/TT-BYT | Hanoi, 02 June 2010 |
CIRCULAR
ON PROMULGATION OF THE NATIONAL TECHNICAL REGULATION FOR FLUID MILK PRODUCTS
MINISTER OF HEALTH
Pursuant to the Law on Technical standards and regulations dated 29 June 2006 and the Government's Decree No. 127/2007/ND-CP dated 01 August 2007 on details for the enforcement of certain articles of the Law on Technical standards and regulations;
Pursuant to the Ordinance on Food hygiene and safety dated 07 August 2003 and the Government’s Decree No. 163/2004/ND-CP dated 07 September 2004 on details for the enforcement of certain articles of the Ordinance on Food hygiene and safety;
Pursuant to the Government’s Decree No. 188/2007/ND-CP dated 27 December 2007 on the functions, missions, powers and organizational structure of Ministry of Health;
At the requests of the Head of the Food Hygiene and Safety Administration, Head of the Science and Education Department, and Head of the Legal Department.
REGULATES:
Article 1. This Circular is enclosed with the national technical regulation QCVN 5-1:2010/BYT for fluid milk products.
Article 2. This Circular comes into force as of 01 January 2011.
Article 3. Head of the Food Hygiene and Safety Administration, Heads of agencies under the Ministry of Health, agencies of the Ministry of Health, Directors of Health Departments of provinces and centrally affiliated cities and concerned entities are responsible for enforcing this Circular.
| FOR THE MINISTER |
QCVN 5-1:2010/BYT
NATIONAL TECHNICAL REGULATION FOR FLUID MILK PRODUCTS
Preamble
QCVN 5-1:2010/BYT is compiled by the Committee for drafting of National technical regulations for food hygiene and safety for milk and milk products, is presented by the Food Hygiene and Safety Administration, and is promulgated under the Circular No. 30/2010/TT-BYT dated 02 June 2010 by Minister of Health.
NATIONAL TECHNICAL REGULATION FOR FLUID MILK PRODUCTS
1. GENERAL
1.1. Scope of regulation
This Regulation defines food safety norms and administrative requirements for fluid milk products including pasteurized whole milk, pasteurized milk, sterilized whole milk, sterilized milk, evaporated milk (condensed milk), evaporated milk (condensed milk) with vegetable fat added.
This Regulation shall not govern formula milk products for children of up to 36 months of age, infant formula milk for special medical purposes and dietary supplements.
1.2. Regulated entities
This Regulation shall apply to:
a) Organizations and individuals importing, producing and selling fluid milk products in Vietnam;
b) Entities concerned.
1.3. Terminology
In this Regulation, the following words and phrases are construed as follows:
1.3.1. Pasteurized whole milk
Products that contain solely pasteurized fresh milk without any milk constituents or additives.
1.2.3. Pasteurized fresh milk
Products that are pasteurized and mainly made of fresh milk, without any milk constituents, though permissibly added with sugar and other ingredients such as juices, cocoa, coffee or food additives.
1.3.3. Sterilized whole milk
Products that contain solely sterilized fresh milk without any milk constituents or additives.
1.2.3. Sterilized fresh milk
Products that are sterilized and mainly made of fresh milk, without any milk constituents, though permissibly added with sugar and other ingredients such as juices, cocoa, coffee or food additives.
1.3.5. Sterilized milk
Products that contain powder milk or evaporated milk or fresh milk added with an adequate portion of water to reconstitute the ratio of water and dried material to a satisfactory extent. Sterilized milk shall be the primary content with probable addition of sugar, juices, cocoa, coffee and food additives.
1.3.6. Evaporated (condensed) milk
Milk products from which water is partially removed or which contain more or less milk constituents though preserving the composition and characteristics of such products and maintaining the original milk ingredient's ratio of whey protein to casein. Sugar and food additives may be added.
1.3.7. Evaporated skimmed milk added with vegetable fat (condensed milk added with vegetable fat)
Milk products whose main content is skimmed milk supplemented with water and vegetable fat. Sugar and food additives may be added.
2. TECHNICAL REQUIREMENTS
2.1. Food safety norms for fluid milk products
2.1.1. Physicochemical norms are defined in Annex I of this Regulation.
2.1.2. Maximum limit of contaminants is specified in Annex II of this Regulation.
2.1.3. Microbial norms are prescribed in Annex III of this Regulation.
2.1.4. The list of permissible food additives pertinent to current regulations.
2.1.5 It is permissible to employ testing measures with precision equivalent to that of methods defined by norm in Annex I, Annex II and Annex III of this Regulation.
2.1.6. Codes and full names of sampling approaches and testing methods are indicated in Annex IV of this Regulation.
2.1.7. Ministry of Health shall regulate tests for norms, whose testing methods are not available in this Regulation, according to accredited measures being employed locally or abroad.
2.2. Labeling
The labeling of fluid milk products must conform to the Government's Decree No. 89/2006/ND-CP dated 30 August 2006 on product label and written guidelines.
3. MANAGEMENT REGULATIONS
3.1. Announcement of conformity
3.1.1. The conformity of fluid milk products imported, produced and sold domestically must be announced according to this Regulation.
3.1.2. Methods and procedures for announcement of conformity shall be governed by the Regulation on certification and announcement of conformity and conformance under the Decision No. 24/2007/QĐ-BKHCN dated 28 September 2007 by Minister of Science and Technology and as per the laws.
3.2. Inspection of fluid milk products
The inspection of the quality, hygiene and safety of fluid milk products must abide by the laws.
4. RESPONSIBILITIES OF ORGANIZATIONS AND INDIVIDUALS
4.1. Importers and producers of fluid milk products must announce their conformity to technical requirements in this Regulation and register such announcements with competent government authorities as specified by the Ministry of Health. Quality, hygiene and safety of the products must be maintained according to such announcements.
4.2. Entities can only import, produce and sell fluid milk products when they complete the registration of the announcement of conformity and maintain quality, hygiene, safety and labeling according to the laws.
5. ENFORCEMENT
5.1. Food Hygiene and Safety Administration shall lead and coordinate with relevant authorities to guide and organize the enforcement of this Regulation.
5.2. Food Hygiene and Safety Administration, according to its managerial devoirs, shall be responsible for proposing to the Ministry of Health the amendments and supplements to this Regulation.
5.3. If amendments, supplements or replacements of standards and regulations stated in this Regulation occur, such revisions shall govern.
ANNEX I
PHYSICOCHEMICAL NORMS FOR FLUID MILK PRODUCTS
Entry | Regulated limit | Testing method | Category of norms 1) |
I. Pasteurized whole milk and pasteurized fresh milk | |||
1. Milk protein, % by weight, not lower than | 2.7 | TCVN 7774:2007 (ISO 5542:1984), TCVN 8099-1:2009 (ISO 8968-1:2001), TCVN 8099-5:2009 (ISO 8968-5:2001) | A |
2. Density at 20oC is not lower than | 1.026 | TCVN 5860:2007 | A |
3. Pasteurization effect (phosphatase test) | Tested and passed | TCVN 5860:2007 | A |
II. Sterilized whole milk | |||
1. Milk protein, % by weight, not lower than | 2.7 | TCVN 7774:2007 (ISO 5542:1984), TCVN 8099-1:2009 (ISO 8968-1:2001), TCVN 8099-5:2009 (ISO 8968-5:2001) | A |
2. Density at 20oC is not lower than | 1.026 | TCVN 7028:2009 | A |
III. Evaporated (condensed) milk | |||
1. Milk protein content, % by weight of non-fat dried material, not lower than | 34 | TCVN 7774:2007 (ISO 5542:1984), TCVN 8099-1:2009 (ISO 8968-1:2001), TCVN 8099-5:2009 (ISO 8968-5:2001) | A |
1) Category A: tests are required for assessment of conformity. |
ANNEX II
LIMITATION OF CONTAMINANTS IN FLUID MILK PRODUCTS
Entry | Maximum limit | Testing method | Category of norms 2) |
I. Heavy metal | |||
1. Lead in milligram per kilogram of products as stated in Clauses 1.3.1 to 1.3.5 or in milligram per kilogram of prepared mixture of products as defined in Clause 1.3.6 and 1.3.7. | 0.02 | TCVN 7933:2008 (ISO 6733:2006), TCVN 7929:2008 (EN 14083:2003) | A |
2. Tin (for products stored in tin coated containers), mg/kg | 250 | TCVN 7730:2007 (ISO/TS 9941:2005), TCVN 8110:2009 (ISO 14377:2002), TCVN 7788:2007 | A |
3. Antimony, mg/kg | 1.0 | TCVN 8132:2009 | B |
4. Arsenic, mg/kg | 0.5 | TCVN 7601:2007 | B |
5. Cadmium, mg/kg | 1.0 | TCVN 7603:2007, TCVN 7929:2008 (EN 14083:2003) | B |
6. Mercury, mg/kg | 0.05 | TCVN 7993:2008 (EN 13806:2002) | B |
II. Mycotoxin |
|
|
|
1. Aflatoxin M1, mg/kg | 0.5 | TCVN 6685:2009 (ISO 14501:2007) | A |
III. Melamine |
|
|
|
1. Melamine, mg/kg | 2.5 | Common technical regulation for enumeration of melamine in foodstuffs (Decision No. 4143/QD-BYT) | B |
IV. Residue of veterinary medicines, mg/kg |
|
| |
1. Benzylpenicillin/ Procaine benzylpenicillin | 4 | TCVN 8106:2009 (ISO/TS 26844:2006); AOAC 988.08 | A |
2. Clortetracyclline/ Oxytetracycline/ Tetracycline | 100 | TCVN 8106:2009 (ISO/TS 26844:2006); AOAC 995.04 | A |
3. Dihydrostreptomycin/ Streptomycin | 200 | TCVN 8106:2009 (ISO/TS 26844:2006); AOAC 988.08 | A |
4. Gentamicin | 200 | TCVN 8106:2009 (ISO/TS 26844:2006) | A |
5. Spiramycin | 200 | TCVN 8106:2009 (ISO/TS 26844:2006) | A |
6. Ceftiofur | 100 | TCVN 8106:2009 (ISO/TS 26844:2006) | B |
7. Clenbuterol | 50 |
| B |
8. Cyfluthrin 3) | 40 | TCVN 8101:2009 (ISO 8260:2008) | B |
9. Cyhalothrin 3) | 30 | AOAC 998.01 | B |
10. Cypermethrin and Alpha cypermethrin | 100 | US FDA PAM, Vol. I, Section 304, E4/C2, C4; TCVN 8101:2009 (ISO 8260:2008)
| B |
11. Deltamethrin 3) | 30 | TCVN 8101:2009 (ISO 8260:2008) | B |
12. Diminazen | 150 |
| B |
13. Doramectin | 15 |
| B |
14. Eprinomectin | 20 |
| B |
15. Febantel/ Fenbendazole/ Oxfendazole | 100 |
| B |
16. Imidocarb | 50 |
| B |
17. Isometamidium | 100 |
| B |
18. Ivermectin | 10 |
| B |
19. Lincomycin | 150 | AOAC 988.08 | B |
20. Neomycin | 1500 | TCVN 8106:2009 (ISO/TS 26844:2006) | B |
21. Pirlimycin | 200 |
| B |
22. Spectinomycin | 200 |
| B |
23. Sulfadimidine | 25 | AOAC 992.21 | B |
24. Thiabendazole 3) | 100 |
| B |
25. Triclorfon (Metrifonate) 3) | 50 |
| B |
V. Residue of pesticides 4), mg/kg | |||
V.1. Pesticides soluble in water or partially soluble in fat | |||
1. Endosulfan | 0.01 | TCVN 7082:2002 (ISO 3890:2000), part 1 and part 2; TCVN 8170:2009 (EN 1528:1996), parts 1, 2, 3 and 4 | A |
2. 2,4-D | 0.01 | US FDA PAM, Vol. I, Section 402, E1 | B |
3. Abamectin | 0.005 |
| B |
4. Acephate | 0.02 | AOAC 970.52 | B |
5. Aldicarb | 0.01 | US FDA PAM, Vol. I, Section 401, E1+DL1 | B |
6. Aminopyralid | 0.02 |
| B |
7. Amitraz | 0.01 |
| B |
8. Bentazon | 0.05 |
| B |
9. Bifenazate | 0.01 |
| B |
10. Bifenthrin | 0.05 | AOAC 970.52 | B |
11. Bitertanol | 0.05 |
| B |
12. Carbaryl | 0.05 | AOAC 964.18; US FDA PAM, Vol. I, Section 401, E1+DL1 | B |
13. Carbendazim | 0.05 |
| B |
14. Carbofuran | 0.05 | US FDA PAM, Vol. I, Section 401, E1, DL1 | B |
15. Carbosulfan | 0.03 |
| B |
16. Chlormequat | 0.5 |
| B |
17. Chlorpropham | 0.0005 | US FDA PAM, Vol. I, Section 304, E4, C1-C4 | B |
18. Chlorpyrifos | 0.02 | TCVN 8101:2009 (ISO 8260:2008) | B |
19. Chlorpyrifos-methyl | 0.01 | TCVN 8101:2009 (ISO 8260:2008) | B |
20. Clethodim | 0.05 |
| B |
21. Clofentezine | 0.05 |
| B |
22. Cyhexatin | 0.05 |
| B |
23. Cyprodinil | 0.0004 |
| B |
24. Cyromazine | 0.01 |
| B |
25. Dichlorvos | 0.02 | TCVN 8101:2009 (ISO 8260:2008) | B |
26. Difenoconazole | 0.005 |
| B |
27. Dimethenamid-p | 0.01 |
| B |
28. Dimethipin | 0.01 |
| B |
29. Dimethoate | 0.05 | AOAC 970.52 | B |
30. Dimethomorph | 0.01 |
| B |
31. Diquat | 0.01 |
| B |
32. Disulfoton | 0.01 |
| B |
33. Dithiocarbamate | 0.05 |
| B |
34. Ethephon | 0.05 |
| B |
35. Ethoprophos | 0.01 | US FDA PAM, Vol. I, Section 304, E4, C1, C3 | B |
36. Fenamiphos | 0.005 |
| B |
37. Fenbuconazole | 0.05 |
| B |
38. Fenbutatin-oxide | 0.05 |
| B |
39. Fenpropimorph | 0.01 |
| B |
40. Fipronil | 0.02 | US FDA PAM, Vol. I, Section 304, E4, C1-C4 | B |
41. Fludioxonil | 0.01 |
| B |
42. Flutolanil | 0.05 |
| B |
43. Glufosinate ammonium | 0.02 |
| B |
44. Imidacloprid | 0.02 |
| B |
45. Indoxacarb | 0.1 |
| B |
46. Kresoxim-methyl | 0.01 |
| B |
47. Lindane | 0.01 | AOAC 970.52 | B |
48. Methamidophos | 0.02 |
| B |
49. Methidathion | 0.001 | US FDA PAM, Vol. I, Section 304, E4, C2, C4 | B |
50. Methomyl | 0.02 | US FDA PAM, Vol. I, Section 401, E1, DL1 | B |
51. Methoxyfenozide | 0.01 |
| B |
52. Myclobutanil | 0.01 |
| B |
53. Novaluron | 0.4 |
| B |
54. Oxamyl | 0.02 | US FDA PAM, Vol. I, Section 401, E1, DL1 | B |
55. Oxydemeton-methyl | 0.01 |
| B |
56. Paraquat | 0.005 |
| B |
57. Penconazole | 0.01 |
| B |
58. Pirimicarb | 0.01 |
| B |
59. Pirimiphos-methyl | 0.01 | TCVN 8101:2009 (ISO 8260:2008) | B |
60. Prochloraz | 0.05 |
| B |
61. Profenofos | 0.01 | US FDA PAM, Vol. I, Section 304, E4, C1, C3 | B |
62. Propamocarb | 0.01 |
| B |
63. Propiconazole | 0.01 |
| B |
64. Pyraclostrobin | 0.03 |
| B |
65. Pyrimethanil | 0.01 | US FDA PAM, Vol. I, Section 304, E4, C1-C4 | B |
66. Quinoxyfen | 0.01 |
| B |
67. Spinosad | 1 |
| B |
68. Tebuconazole | 0.01 |
| B |
69. Tebufenozide | 0.01 |
| B |
70. Terbufos | 0.01 | US FDA PAM, Vol. I, Section 304, C1-C4 | B |
71. Thiacloprid | 0.05 |
| B |
72. Triadimefon | 0.01 | US FDA PAM, Vol. I, Section 304, C1, C3 | B |
73. Triadimenol | 0.01 |
| B |
74. Trifloxystrobin | 0.02 |
| B |
75. Vinclozolin | 0.05 | US FDA PAM, Vol. I, Section 304, C1-C3; E1-E5+C6 | B |
V.2. Pesticides soluble in fat 5) | |||
1. Aldrin and dieldrin | 0.006 | TCVN 7082:2002 (ISO 3890:2000), part 1 and part 2; TCVN 8101:2009 (ISO 8260:2008); TCVN 8170:2009 (EN 1528:1996), parts 1, 2, 3 and 4 | A |
2. Cyfluthrin 6) | 0.04 | TCVN 8101:2009 (ISO 8260:2008) | A |
3. Chlordane | 0.002 | TCVN 7082:2002 (ISO 3890:2000), part 1 and part 2; TCVN 8170:2009 (EN 1528:1996), parts 1, 2, 3 and 4 | B |
4. Cypermethrin | 0.05 | US FDA PAM, Vol. I, Section 304, E4/C2, C4; | B |
5. DDT | 0.02 | TCVN 7082:2002 (ISO 3890:2000), part 1 and part 2; TCVN 8170:2009 (EN 1528:1996), parts 1, 2, 3 and 4 | A |
6. Deltamethrin 6) | 0.05 | TCVN 8101:2009 (ISO 8260:2008) | B |
7. Diazinon | 0.02 | TCVN 8101:2009 (ISO 8260:2008) | B |
8. Dicofol | 0.1 | TCVN 8101:2009 (ISO 8260:2008) | B |
9. Diflubenzuron | 0.02 |
| B |
10. Diphenylamine | 0.0004 |
| B |
11. Famoxadone | 0.03 |
| B |
12. Fenhexamid | 0.01 |
| B |
13. Fenpropathrin | 0.1 | US FDA PAM Vol. I, Section 304, E4, C1-C4 | B |
14. Fenpyroximate | 0.005 |
| B |
15. Fenvalerate | 0.1 | TCVN 8101:2009 (ISO 8260:2008); AOAC 998.01 | B |
16. Flumethrin | 0.05 |
| B |
17. Flusilazole | 0.05 |
| B |
18. Heptachlor | 0.006 | TCVN 7082:2002 (ISO 3890:2000), part 1 and part 2; TCVN 8170:2009 (EN 1528:1996), parts 1, 2, 3 and 4 | B |
19. Methoprene | 0.1 |
| B |
20. Permethrin | 0.1 | TCVN 8101:2009 (ISO 8260:2008) | B |
21. Phorate | 0.01 | US FDA PAM Vol. I, Section 304, C2, C4 | B |
22. Piperonyl Butoxide | 0.05 | US FDA PAM Vol. I, Section 401, E1, DL2 | B |
23. Propargite | 0.1 | US FDA PAM Vol. I, Section 304, E4+C6 | B |
2) Category A: tests are required for assessment of conformity. Category B: though tests are not required for assessment of conformity, entities producing, importing and processing fluid milk products must abide by requirements for norms under Category B. 3) Also used as pesticide 4) By reference to testing methods in TCVN 5142:2008 (CODEX STAN 229-1993, Rev.1-2003) 5) This limit applies to pasteurized and sterilized milk products as defined in Clause 1.3.1 to 1.3.5. If milk products have the fat content less than 2%, the maximum limits shall be half of those defined in this Regulation. If milk products have the fat content at 2% by weight or higher, the limits shall be at 25 times those defined in this Regulation according to the fat content in milk products. 6) Also used as veterinary medicines. |
ANNEX III
MICROBIAL NORMS OF FLUID MILK PRODUCTS
Entry | Sampling | Limit | Testing method | Category of norms 11) | ||
n 7) | c 8) | m 9) | M 10) | |||
1. Enterobacteriaceae | 5 | 2 | < 1 CFU/ml | 5 CFU/ml | TCVN 5518-1:2007 (ISO 21528-1:2004) | A |
2. Listeria monocytogenes (for instant milk products) | 5 | 0 | 100 CFU/ml | TCVN 7700-2:2007 (ISO 11290-2:1998, With amd.1:2004) | A | |
7) n: quantity of tested samples from a batch of products 8) c: maximum amount of samples tolerable or containing the microorganism m in excess of the limit. If the number of failed samples exceeds this tolerance, the batch of products shall be disqualified. 9) m: maximum quantity or level of bacteria in 1 gram of a milk product. Excess may be permissible or unacceptable. 10) M: maximum level of microorganism as the threshold of satisfactory and failed quality. 11) Category A: tests are required for assessment of conformity. |
ANNEX IV
LIST OF TESTING METHODS FOR FOOD SAFETY NORMS FOR FLUID MILK PRODUCTS
I. Sampling
1. TCVN 6400 (ISO 707) Milk and milk products - Guidance on sampling.
II. Testing methods for physicochemical norms
1. TCVN 5860:2007 Pasteurize fresh milk
2. TCVN 7028:2009 Sterilized fresh milk
3. TCVN 7774:2007 (ISO 5542:1984) Milk - Determination of protein content -- Amido black dye-binding method (Routine method)
4. TCVN 8082:2009 (ISO 6731:1989) Milk, cream and evaporated milk -- Determination of total solids content (Reference method)
5. TCVN 8099-1:2009 (ISO 8968-1:2001) Milk -- Determination of nitrogen content -- Part 1: Kjeldahl method
6. TCVN 8099-5:2009 (ISO 8968-5:2001 Milk -- Determination of nitrogen content -- Part 5: Determination of protein-nitrogen content
III. Testing methods for contaminants
III.1. Heavy metal
1. TCVN 7601:2007 Foodstuffs – Determination of arsenic content by silver diethyldithiocarbamate method
2. TCVN 7603:2007 Foods – Determination of cadmium content by atomic absorption spectrophotometric method
3. TCVN 7730:2007 (ISO/TS 9941:2005) Milk and canned evaporated milk - Determination of tin content - Spectrometric method
4. TCVN 7788:2007 Canned foods - Determination of tin content by atomic absorption spectrophotometric method
5. TCVN 7929:2008 (EN 14083:2003) Foodstuffs - Determination of trace elements - Determination of lead, cadmium, chromium and molybdenum by graphite furnace atomic absorption spectrometry (GFAAS) after pressure digestion
6. TCVN 7933:2008 (ISO 6733:2006) Milk and milk products - Determination of lead content - Graphite furnace atomic absorption spectrometric method
7. TCVN 7993:2008 (EN 13806:2002) Foodstuffs - Determination of trace elements - Determination of mercury by cold-vapour atomic absorption spectrometry (CVAAS) after pressure digestion
8. TCVN 8110:2009 (ISO 14377:2002) Canned evaporated milk – Determination of tin content – Method using graphite furnace atomic absorption spectrometry
9. TCVN 8132:2009 Foodstuffs – Determination of antimony content by spectrophotometric method
III.2. Mycotoxin
1. TCVN 6685:2009 (ISO 14501:2007) Milk and milk powder - Determination of aflatoxin M1 content - Clean-up by immunoaffinity chromatography and determination by high-performance liquid chromatography
III.3. Melamine
1. Common technical regulation on enumeration of melamine in foodstuffs, as enclosed to the Decision No. 4143/QĐ-BYT dated 22 October 2008
III.4. Residue of veterinary medicines
1. TCVN 8101:2009 (ISO 8260:2008) Milk and milk products - Determination of organochlorine pesticides and polychlorobiphenyls - Method using capillary gas-liquid chromatography with electron-capture detection
2. TCVN 8106:2009 (ISO/TS 26844:2006) Milk and milk products -- Determination of antimicrobial residues -- Tube diffusion test
3. AOAC 988.08 Antimicrobial Drugs in Milk. Microbial Receptor Assay (antibiotics in milk)
4. AOAC 992.21 Sulfamethazine Residues in Raw Bovine Milk (Residue of sulfamethazine in raw bovine milk)
5. AOAC 995.04 Multiple Tetracycline Residues in Milk Metal Chelate Affinity-Liquid Chromatographic Method (Residue of tetracycline in milk) Metal Chelate Affinity-Liquid Chromatographic Method
6. AOAC 995.09 Chlortetracycline, Oxytetracycline, and Tetracycline in Edible Animal Tissues Liquid Chromatographic Method (Chlortetracycline, oxytetracycline and tetracycline in cattle meat)
7. AOAC 998.01 Synthetic Pyrethroids in Agricultural Products Multiresidue. Gas Chromatography Method (Synthetic pyrethroid in agricultural products)
8. Pesticide Analytical Manual (PAM), Food and Drug Administration, Washington, D.C., USA, Vol. I, 3rd edition, Section 304
9. Pesticide Analytical Manual (PAM), Food and Drug Administration, Washington, D.C., USA, Vol. I, 3rd edition, Section 401
10. Pesticide Analytical Manual (PAM), Food and Drug Administration, Washington, D.C., USA, Vol. I, 3rd edition, Section 402
III.5. Residue of pesticides
1. TCVN 5142:2008 (CODEX STAN 229-1993, Rev.1-2003) Analysis of residue of pesticides - Recommended methods.
2. TCVN 7082-1:2002 (ISO 3890-1:2000) Milk and milk products - Determination of residues of organochlorine compounds (pesticides) - Part 1: General considerations and extraction methods
3. TCVN 7082-2:2002 (ISO 3890-2:2000) Milk and milk products - Determination of residues of organochlorine compounds (pesticides) - Part 2: Test methods for crude extract purification and confirmation
4. TCVN 8101:2009 (ISO 8260:2008) Milk and milk products - Determination of organochlorine pesticides and polychlorobiphenyls - Method using capillary gas-liquid chromatography with electron-capture detection
5. TCVN 8170-1:2009 (EN 1528-1:1996) Fatty food - Determination of pesticides and polychlorinated biphenyls (PCBs) - Part 1: General
6. TCVN 8170-2:2009 (EN 1528-2:1996) Fatty food - Determination of pesticides and polychlorinated biphenyls (PCBs) - Part 2: Extraction of fat, pesticides and PCBs, and determination of fat content
7. TCVN 8170-3:2009 (EN 1528-3:1996) Fatty food - Determination of pesticides and polychlorinated biphenyls (PCBs) - Part 3: Clean-up methods
8. TCVN 8170-4:2009 (EN 1528-4:1996) Fatty food - Determination of pesticides and polychlorinated biphenyls (PCBs) - Part 4: Determination, confirmatory tests, miscellaneous
9. AOAC 964.18 Carbaryl Pesticide Residues Colorimetric Method (Residue of carbaryl)
10. AOAC 970.52 Organochlorine and Organophosphorus Pesticide Residues General Multiresidue Method (Content of organochlorine and organophosphorus)
IV. Testing methods for microbial norms
1. TCVN 5518-1:2007 (ISO 21528-1:2004) Microbiology of food and animal feeding stuffs -Horizontal methods for the detection and enumeration of Enterobacteriaceae - Part 1: Detection and enumeration by MPN technique with pre-enrichment
2. TCVN 7700-2:2007 (ISO 11290-2:1998, With amd.1:2004) Microbiology of food and animal feeding stuffs - Horizontal method for the detection and enumeration of Listeria monocytogenes - Part 2: Enumeration method
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